Fundamentals of Analytical Chemistry, 10th Edition Douglas A Skoog, Donald M West, F James Holler, Stanley R Crouch

Cover
Contents in Brief
Contents
Preface
Chapter 1: The Nature of Analytical Chemistry
	1A: The Role of Analytical Chemistry
	1B: Quantitative Analytical Methods
	1C: A Typical Quantitative Analysis
	1D: An Integral Role for Chemical Analysis: Feedback Control Systems
Part I: Quality Of Analytical Measurements
	Chapter 2: Calculations Used in Analytical Chemistry
		2A: Some Important Units of Measurement
		2B: Solutions and Their Concentrations
		2C: Chemical Stoichiometry
	Chapter 3: Precision and Accuracy of Chemical Analyses
		3A: Some Important Terms
		3B: Systematic Errors
	Chapter 4: Random Errors in Chemical Analysis
		4A: The Nature of Random Errors
		4B: Statistical Treatment of Random Errors
		4C: Standard Deviation of Calculated Results
		4D: Reporting Computed Data
	Chapter 5: Statistical Data Treatment and Evaluation
		5A: Confidence Intervals
		5B: Statistical Aids to Hypothesis Testing
		5C: Analysis of Variance
		5D: Detection of Gross Errors
	Chapter 6: Sampling, Standardization, and Calibration
		6A: Analytical Samples and Methods
		6B: Sampling
		6C: Automated Sample Handling
		6D: Standardization and Calibration
		6E: Figures of Merit for Analytical Methods
Part II: Chemical Equilibria
	Chapter 7: Aqueous Solutions and Chemical Equilibria
		7A: The Chemical Composition of Aqueous Solutions
		7B: Chemical Equilibrium
		7C: Buffer Solutions
	Chapter 8: Effect of Electrolytes on Chemical Equilibria
		8A: The Effect of Electrolytes on Chemical Equilibria
		8B: Activity Coefficients
	Chapter 9: Solving Equilibrium Problems for Complex Systems
		9A: Solving Multiple-Equilibrium Problems Using a Systematic Method
		9B: Calculating Solubilities by the Systematic Method
		9C: Separation of Ions by Control of the Concentration of the Precipitating Agent
Part III: Classical Methods of Analysis
	Chapter 10: Gravimetric Methods of Analysis
		10A: Precipitation Gravimetry
		10B: Calculation of Results from Gravimetric Data
		10C: Applications of Gravimetric Methods
	Chapter 11: Titrations in Analytical Chemistry
		11A: Some Terms Used in Volumetric Titrations
		11B: Standard Solutions
		11C: Volumetric Calculations
		11D: Gravimetric Titrations
		11E: Titration Curves
	Chapter 12: Principles of Neutralization Titrations
		12A: Solutions and Indicators for Acid-Base Titrations
		12B: Titration of Strong Acids and Bases
		12C: Titration Curves for Weak Acids
		12D: Titration Curves for Weak Bases
		12E: The Composition of Solutions During Acid-Base Titrations
	Chapter 13: Complex Acid-Base Systems
		13A: Mixtures of Strong and Weak Acids or Strong and Weak Bases
		13B: Polyfunctional Acids and Bases
		13C: Buffer Solutions Involving Polyprotic Acids
		13D: Calculation of the pH of Solutions of NaHA
		13E: Titration Curves for Polyfunctional Acids
		13F: Titration Curves for Polyfunctional Bases
		13G: Titration Curves for Amphiprotic Species
		13H: Composition of Polyprotic Acid Solutions as a Function of pH
	Chapter 14: Applications of Neutralization Titrations
		14A: Reagents for Neutralization Titrations
		14B: Typical Applications of Neutralization Titrations
	Chapter 15: Complexation and Precipitation Reactions and Titrations
		15A: The Formation of Complexes
		15B: Titrations with Inorganic Complexing Agents
		15C: Organic Complexing Agents
		15D: Aminocarboxylic Acid Titrations
Part IV: Electrochemical Methods
	Chapter 16: Introduction to Electrochemistry
		16A: Characterizing Oxidation/Reduction Reactions
		16B: Electrochemical Cells
		16C: Electrode Potentials
	Chapter 17: Applications of Standard Electrode Potentials
		17A: Calculating Potentials of Electrochemical Cells
		17B: Determining Standard Potentials Experimentally
		17C: Calculating Redox Equilibrium Constants
		17D: Constructing Redox Titration Curves
		17E: Oxidation/Reduction Indicators
		17F: Potentiometric End Points
	Chapter 18: Applications of Oxidation/Reduction Titrations
		18A: Auxiliary Oxidizing and Reducing Reagents
		18B: Applying Standard Reducing Agents
		18C: Applying Standard Oxidizing Agents
	Chapter 19: Potentiometry
		19A: General Principles
		19B: Reference Electrodes
		19C: Liquid Junction Potentials
		19D: Indicator Electrodes
		19E: Instruments for Measuring Cell Potential
		19F: Direct Potentiometry
		19G: Potentiometric Titrations
		19H: Potentiometric Determination of Equilibrium Constants
	Chapter 20: Bulk Electrolysis: Electrogravimetry and Coulometry
		20A: The Effect of Current on Cell Potential
		20B: The Selectivity of Electrolytic Methods
		20C: Electrogravimetric Methods
		20D: Coulometric Methods
	Chapter 21: Voltammetry
		21A: Excitation Signals in Voltammetry
		21B: Voltammetric Instrumentation
		21C: Hydrodynamic Voltammetry
		21D: Polarography
		21E: Cyclic Voltammetry
		21F: Pulse Voltammetry
		21G: Applications of Voltammetry
		21H: Stripping Methods
		21I: Voltammetry with Microelectrodes
Part V: Spectrochemical Analysis
	Chapter 22: Introduction to Spectrochemical Methods
		22A: Properties of Electromagnetic Radiation
		22B: Interaction of Radiation and Matter
		22C: Absorption of Radiation
		22D: Emission of Electromagnetic Radiation
	Chapter 23: Instruments for Optical Spectrometry
		23A: Instrument Components
		23B: Ultraviolet/Visible Photometers and Spectrophotometers
		23C: Infrared Spectrophotometers
	Chapter 24: Molecular Absorption Spectrometry
		24A: Ultraviolet and Visible Molecular Absorption Spectroscopy
		24B: Automated Photometric and Spectrophotometric Methods
		24C: Infrared Absorption Spectroscopy
	Chapter 25: Molecular Fluorescence Spectroscopy
		25A: Theory of Molecular Fluorescence
		25B: Effect of Concentration on Fluorescence Intensity
		25C: Fluorescence Instrumentation
		25D: Applications of Fluorescence Methods
		25E: Molecular Phosphorescence Spectroscopy
		25F: Chemiluminescence Methods
	Chapter 26: Atomic Spectroscopy
		26A: Origins of Atomic Spectra
		26B: Production of Atoms and Ions
		26C: Atomic Emission Spectrometry
		26D: Atomic Absorption Spectrometry
		26E: Atomic Fluorescence Spectrometry
	Chapter 27: Mass Spectrometry
		27A: Principles of Mass Spectrometry
		27B: Mass Spectrometers
		27C: Atomic Mass Spectrometry
		27D: Molecular Mass Spectrometry
Part VI: Kinetics And Separations
	Chapter 28: Kinetic Methods of Analysis
		28A: Rates of Chemical Reactions
		28B: Determining Reaction Rates
		28C: Applications of Kinetic Methods
	Chapter 29: Introduction to Analytical Separations
		29A: Separation by Precipitation
		29B: Separation of Species by Distillation
		29C: Separation by Extraction
		29D: Separating Ions by Ion Exchange
		29E: Chromatographic Separations
	Chapter 30: Gas Chromatography
		30A: Instruments for Gas-Liquid Chromatography
		30B: Gas Chromatographic Columns and Stationary Phases
		30C: Applications of Gas-Liquid Chromatography
		30D: Gas-Solid Chromatography
	Chapter 31: High-Performance Liquid Chromatography
		31A: Instrumentation
		31B: Partition Chromatography
		31C: Adsorption Chromatography
		31D: Ion Chromatography
		31E: Size-Exclusion Chromatography
		31F: Affinity Chromatography
		31G: Chiral Chromatography
		31H: Comparison of High-Performance Liquid Chromatography and Gas Chromatography
	Chapter 32: Miscellaneous Separation Methods
		32A: Supercritical Fluid Separations
		32B: Planar Chromatography
		32C: Capillary Electrophoresis
		32D: Capillary Electrochromatography
		32E: Field-Flow Fractionation
Part VII: Practical Aspects Of Chemical Analysis
	Chapter 33: The Analysis of Real Samples
		33A: Real Samples
		33B: Choice of Analytical Method
		33C: Accuracy in the Analysis of Complex Materials
	Chapter 34: Preparing Samples for Analysis
		34A: Preparing Laboratory Samples
		34B: Moisture in Samples
		34C: Determining Water in Samples
	Chapter 35: Decomposing and Dissolving the Sample
		35A: Sources of Error in Decomposition and Dissolution
		35B: Decomposing Samples with Inorganic Acids in Open Vessels
		35C: Microwave Decompositions
		35D: Combustion Methods for Decomposing Organic Samples
		35E: Decomposing Inorganic Materials with Fluxes
	Chapter 36: Chemicals, Apparatus, and Unit Operations of Analytical Chemistry
		36A: Selecting and Handling Reagents and Other Chemicals
		36B: Cleaning and Marking  of Laboratory Ware
		36C: Evaporating Liquids
		36D: Measuring Mass
		36E: Equipment and Manipulations  Associated with Weighing
		36F: Filtration and Ignition of Solids
		36G: Measuring Volume
		36H: Calibrating Volumetric Glassware
		36I: The Laboratory Notebook
		36J: Safety in the Laboratory
	Chapter 37 Selected Methods of Analysis
		37A: An Introductory Experiment
		37B: Gravimetric Methods of Analysis
		37C: Neutralization Titrations
		37D: Precipitation Titrations
		37E: Complex-Formation Titrations with EDTA
		37F: Titrations with Potassium Permanganate
		37G: Titrations with Iodine
		37H: Titrations with Sodium Thiosulfate
		37I: Titrations with Potassium Bromate
		37J: Potentiometric Methods
		37K: Electrogravimetric Methods
		37L: Coulometric Titrations
		37M: Voltammetry
		37N: Methods Based on the Absorption of Radiation
		37O: Molecular Fluorescence
		37P: Atomic Spectroscopy
		37Q: Application of Ion-Exchange Resins
Glossary
Appendix 1:The Literature Of Analytical Chemistry
Appendix 2: Solubility Product Constants at 25°C
Appendix 3: Acid Dissociation Constants at 25°C
Appendix 4: Formation Constants at 25°C
Appendix 5: Standard and Formal Electrode Potentials
Appendix 6: Use of Exponential Numbers and Logarithms
Appendix 7: Volumetric Calculations Using Normality and Equivalent Weight
Appendix 8: Compounds Recommended for the Preparation of Standard Solutions of Some Common Elements
Appendix 9: Derivation of Error Propagation Equations
Answers to Selected Questions and Problems
Index
Copyright
Title Page
Dedication
Contents
Chapter 1: ‘I’m thinking’ – Oh, but are you?
Chapter 2: Renegade perception
Chapter 3: The Pushbacker sting
Chapter 4: ‘Covid’: The calculated catastrophe
Chapter 5: There is no ‘virus’
Chapter 6: Sequence of deceit
Chapter 7: War on your mind
Chapter 8: ‘Reframing’ insanity
Chapter 9: We must have it? So what is it?
Chapter 10: Human 2.0
Chapter 11: Who controls the Cult?
Chapter 12: Escaping Wetiko
Postscript
Appendix: Cowan-Kaufman-Morell Statement on Virus Isolation
Bibliography
Index