Emerging Trends in Synthesis and Catalysis in Chemistry: Proceedings of ETSC 2023

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Springer Proceedings in Materials Series: Volume 51
Emerging Trends in Synthesis and Catalysis in Chemistry: Proceedings of ETSC 2023
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Preface
Contents
About the Editors
Impurity Profiling of Antihyperglycemic Drug-Sitagliptin
	1. Introduction
	2. Synthesis of API
	3. Impurities of Sitagliptin:
	4. Synthesis of Acid Impurity
		4.1 Alkene Impurity
		4.2 Cyclohexyl Impurity:
		4.3 Enantiomer Impurity
	5. Detection of Sitagliptin and Its Impurities by HPLC and GC–MS
	6. Conclusion
	References
Anticancer and Antimicrobial Studies of Dibutyl(hexadecanoyloxy)stannyl Hexadecanoate
	1. Introduction
	2. Materials and Method
		2.1 Chemicals
		2.2 Instruments
		2.3 Experimental Method
	3. Results and Discussion
		3.1 Study of Physical Properties
		3.2 Characterization
	4. Study of Activity andSuggested Applications of Synthesized Complex
		4.1 In Vitro Antibacterial Test
		4.2 In Silico Antimicrobial Analysis Utilizing the Molecular Docking Software iGEMDOCK
		4.3 Biochemical Function and Process of PDB 1IKQ
		4.4 In Silico Anticancer Studies Using Molecular Docking Software (iGEMDOCK)
		4.5 In Silico Pharmacokinetic Properties Study
	5. Conclusion
	References
Quality Control Methods to Check Phthalates Toxicity in Textile Products
	1. Introduction
	2. Characteristics of Phthalates
		2.1 Advantages of Phthalates
	3. Source of Phthalates
		3.1 Toxicity of Analytes
		3.2 Impact on Human Health
		3.3 Impact on the Environment
		3.4 Animal Risks
	4. Detection Techniques of Phthalate in Textiles
		4.1 Sample Preparation and Extraction Process
		4.2 Principle
		4.3 Detection with GC–MS
	5. Conclusion
	References
Significance of EDTA and Sodium Citrate in Blood Preservation: A Reaction Mechanism with Calcium as Substrate
	1. Introduction
		1.1 EDTA and Other Anticoagulants
		1.2 Composition of Blood
		1.3 Understanding Blood Preservatives: Their Secrets and Pitfalls
		1.4 Mechanism of Coagulation
		1.5 Action Mechanism of EDTA and Sodium Citrate
	2. Discussion
	References
Modern Approaches in the Synthesis of Optically Stimulated Luminescent (OSL) Materials for Dosimetry Applications
	1. Introduction
		1.1 Principle of OSL
		1.2 Properties of Materials Used for OSL Dosimetry
	2. Techniques Used for OSL Detection and Analysis
	3. Overview of Different Types of OSL Materials
	4. Synthesis Methods of OSL Dosimetry
		4.1 Sol–gel Method
		4.2 Co-Precipitation Method
		4.3 Chemical Vapor Deposition (CVD)
		4.4 Microwave-Assisted Synthesis
		4.5 Hydrothermal Synthesis
	5. Characterization of OSL Materials
	6. Applications of OSL Dosimetry
		6.1 Radiation Therapy
		6.2 Personal Radiation Monitoring
		6.3 Environmental Monitoring
		6.4 Radiological Emergencies
		6.5 Medical Imaging
		6.6 Research and Development
	7. Current Challenges and Limitations of OSL Dosimetry
	8. Conclusions
	References
Recent Advances in the Synthesis of Thermoluminescent Materials for Dosimetry Applications
	1. Introduction
	2. Synthesis Techniques of Thermoluminescent Materials
	3. Applications of Thermoluminescent Materials
	4. TLD Badge Application as Personal Dosimetry
	5. Conclusions
	References
Simulation Study of Some Characteristics of Single and Binary Stars Using MAdSTAR, MESA, and NAAP Astronomical Tools
	1. Introduction
	2. Methodology
	3. Results
		3.1 Single Stars with Variable Solar Masses
		3.2 Eclipsing Binary Stars
	4. Discussion of the Results
	5. Conclusions
	References
Variation of In-Situ Partial Pressures of Different Gases Over Southern Polar Region of Moon Utilizing Chandrayaan-2 Data
	1. Introduction
	2. Data Used and Methodology
	3. Results and Discussion
		3.1 Variation of Partial Pressure for JF Season
		3.2 Variation of Partial Pressure for MAM Season
		3.3 Variation of Partial Pressure for JJAS Season
		3.4 Variation of Partial Pressure for on Season
	4. Conclusions
	References
Synthesis of Coumarins by Pechmann Condensation Using Nano-ferrites
	1. Introduction
	2. Experimental and Methods
		2.1 Reagents and Analysis
		2.2 Preparation of Metal Ferrite Nanoparticles
		2.3 Pechmann Condensation for Preparation of 4-Methyl-7-Hydroxy Coumarin
	3. Result and Discussion
	4. Conclusions
	References
Deployment of Solar Energy Concentrators Across the Globe
	1. Introduction
	2. Solar Energy Concentrators
	3. Classification Based on Point or Line Concentration of Sunlight
		3.1 Point Solar Concentrators
		3.2 Line Solar Concentrators
	4. Classification Based on Optical Principle
		4.1 Reflector
		4.2 Refractor
		4.3 Hybrid
		4.4 Luminescent
	5. Deployment of Solar Energy Concentrators
	6. SWOT Analysis of Deployment of Solar Energy Concentrators
		6.1 Strengths
		6.2 Weaknesses
		6.3 Opportunities
		6.4 Threats
	7. Economics of Solar Energy Concentrators
	8. Policies and Regulations
	9. Market Outlook of Solar Concentrators
	10. Competitive Environment for Solar Concentrators
	11. Market Segmentation Research for Solar Concentrators
	12. Conclusion
	References
Analyzing of 6-APA for Synthesis of Amoxicillin
	1. Introduction
	2. Experimental Procedure
	3. Results and Discussion
	4. Calculations
	5. Conclusion
	References
An Innovative Cation Exchange Water Treatment Method Using Zeolite Synthesized from Industrial Waste
	1. Introduction
	2. Experimental
		2.1 Materials
	3. Results and Discussion
	4. Conclusion
	References
Chlor-Alkali Waste in the Production of Wall Tiles: A Sustainable Approach
	1. Introduction
	2. Experimental Methods
		2.1 Materials Used
		2.2 Characterization
	3. Conclusion
	References
MWCNT/TPU Nanocomposites-Based UV Photodetector
	1. Introduction
	2. Experimental Part
		2.1 Materials
	3. Results and Discussion
		3.1 Characteristics of MWCNTs
	4. Conclusion
	References
N-Fluorobenzenesulfonimide (NFSI): A Multipurpose Reagent
	1. Introduction
	2. N-Fluorobenzenesulfonimide as a Nitrogen Compound
		2.1 Reactions with the Transition Metal Using NFSI
		2.2 Metal-Free Chemical Syntheses with NFSI
	3. NFSI as a Fluorine Source
		3.1 Reactions with the Transition Metal Using NFSI
		3.2 Solvent-Mediated Reactions and Metal-Free Reactions with NFSI
	4. Conclusion
	References
A Facile Method for Removal of Methylene Blue Dye from Wastewater Using Biochar-Modified Chitosan Beads
	1. Introduction
	2. Materials and Methods
		2.1 Preparation of Composite
		2.2 Preparation of Methylene Blue Dye Solution
		2.3 Techniques Used
		2.4 Batch Adsorption Studies
		2.5 Adsorption Isotherms
		2.6 Adsorption Kinetics
	3. Results and Discussion
		3.1 Scanning Electron Microscope (SEM)
		3.2 Fourier Transmission Infrared Red (FTIR)
		3.3 Effect of Initial Dye Concentration
		3.4 Effect of pH
		3.5 Effect of Contact Time
		3.6 Effect of Adsorbent Dosage
		3.7 Effect of Temperature
		3.8 Adsorption Isotherms
		3.9 Adsorption Kinetics
		3.10 Thermodynamic Studies
	4. Conclusion
	References
Smart Sustainable Solutions to Mitigate Water Pollution in Yamuna River
	1. Introduction
	2. Sources of Pollution
	3. Government Initiatives to Mitigate Pollution in Yamuna
	4. Conventional Sewage Treatment Process
	5. Nanotechnological Interventions for Wastewater Treatment
		5.1 Nanoparticles: A Potent Alternative to Treat Wastewater
		5.2 Biochar: A Sustainable Adsorbent Material
		5.3 Nanofiltration Membranes for Wastewater Treatment
	6. Construction of Wetlands as a Sustainable Approach to Treat Wastewater
	7. Lessons Learned from Other Countries
	8. Conclusions
	References
Synthesis and Structural Characterization of Schiff Base-Based Transition Metal Complexes
	1. Introduction
	2. Experimental Section
		2.1 Materials and Methods
		2.2 Instrumentation and Characterization
	3. Synthetic Procedure
		3.1 Preparation of Ligand
		3.2 Preparation of [Co(C7H9N3S2)2Cl2]Cl2 Complex
		3.3 Preparation of [Ni(C7H9N3S2)2Cl2]Cl2 Complex
	4. Results and Discussion
		4.1 Preparation and Characterization of Ligand
		4.2 Uv–Visible Spectrum of 2-Acetyl Thiophene Thiosemicarbazone:
		4.3 Preparation and Characterization of the Complexes
	5. Characterization of the Complex
		5.1 Magnetic Behavior of [Co(C7H9N3S2)2Cl2]Cl2 Complex
		5.2 Magnetic Behavior of [Ni(C7H9N3S2)2Cl2]Cl2 Complex
	6. Conductance Behavior of Complex
	7. Spectral Behavior of the Complexes
		7.1 Spectral Behavior of [Co(C7H9N3S2)2Cl2]Cl2 Complex
		7.2 Spectral Behavior of [Ni(C7H9N3S2)2Cl2]Cl2 Complex
	8. Infrared Spectrum of the Complex
	9. Structure of the Complex
	References
Anticancer and Antimicrobial Activities of Schiff Base Ligand and Their Co(II), Cu(II), and Zn(II) Transition Metal Complexes: An Overview
	1. Introduction
	2. Synthesis of Schiff Bases Metal Complex and Their Biological Applications
	3. Conclusion
	References
Design, Synthesis, and Characterization of Some Oxadiazole Derivatives and Their S-Glucosides Bearing Thiazole Scaffold
	1. Introduction
	2. Results and Discussion
	3. Experimental
	4. Concluding Remarks
	References
Microwave-Assisted Synthesis of Monohydroxy Pendant Polybenzobisthiazole Thermoplastic Polymer
	1. Introduction
	2. Experimental
		2.1 Materials and Methods
		2.2 Synthesis of Base Compound 1,3-Bis-(2-Benzothiazoly)-5-Hydroxy Phenylene (3)
		2.3 Synthesis of Poly{(Benzo [1, 2-d: 4, 5-dʹ]-Bisthiazole 2,6-Diyl) 1,3(5–Hydroxy Phenylene)} (5)
	3. Result and Discussion
		3.1 Infrared Analysis
		3.2 I3C Solid NMR
		3.3 Thermal Characterization
	4. Conclusion
	References
Synthesis and Physicochemical Assessment of Anionic Polymeric Surfactant from Palm Oil for Improved Oil Recovery
	1. Introduction
	2. Experimental Procedures
		2.1 Materials
		2.2 Synthesis of Polymeric Methyl Ester Sulphonate
		2.3 Analysis of Polymeric Surfactant Using FTIR
		2.4 Surface Properties of Synthesized Polymeric Surfactant
	3. Results and Discussion
		3.1 Characterization of Polymeric Surfactant by FTIR
		3.2 Physiochemical Properties of Synthesized Polymeric Surfactant
	4. Conclusion
	References
Synthesis of Metal Telluride Nanomaterials and Their Application in Catalysis
	1. Introduction
	2. Experimental Section
		2.1 Materials and Methods
	3. Synthetic Procedure
		3.1 Synthesis of Copper Tellurides Nanoparticles
		3.2 The Procedure of Protection of Protein from Copper-Mediated Oxidative Damage
	4. Result and Discussion
		4.1 Synthesis and Characterization of Copper Telluride Nanoparticles
		4.2 Characterization of Copper Telluride Nanoparticles
	5. Application in Protecting Effect on Protein from Copper Catalyzed Oxidative Damage by Catalyzing/Neutralizing the Copper-Induced Free Radical
	6. Conclusion
	References