Zeolites and Related Microporous Materials: State of the Art 1994 - Proceedings of the 10th International Zeolite Conference, Garmisch-Partenkirchen, Germany, 17-22 July 1994

Content: 
Edited by
Page iii

Copyright page
Page iv

Preface
Pages xxxi-xxxii
J. Weitkamp, H.G. Karge, H. Pfeifer, W. Hölderich

Acknowledgements
Page xxxiii

Committees
Page xxxiv

International Advisory Board
Pages xxxv-xxxvi

Financial Support
Page xxxvii

Zeolites and their Mechanism of Synthesis Original Research Article
Pages 3-21
Eddy J.P. Feijen, Johan A. Martens, Pierre A. Jacobs

The Role of Diquaternary Cations as Directing Agents in Zeolite Synthesis Original Research Article
Pages 23-28
A. Moini, K.D. Schmitt, E.W. Valyocsik, R.F. Polomski

A Study of Guest/Host Energetics for the Synthesis of Cage Structures NON and CHA Original Research Article
Pages 29-36
T.V. Harris, S.I. Zones

Characterization and Catalytic Properties of Zeolite-Supported Platinum-Iridium Bimetallic Catalysts Prepared by Decoration of Platinum with Iridium Original Research Article
Pages 757-763
I.C. Hwang, S.I. Woo

Clustering of Platinum Atoms in Zeolite EMT Supercage: Comprehensive Physicochemical Characterization Original Research Article
Pages 765-772
H. Ihee, R. Ryoo, T. Bécue, C. Potvin, J-M. Manoli, G. Djéga-Mariadassou

XAS Studies on the Interaction of with PtY and PdY Zeolites Original Research Article
Pages 773-780
U. Hatje, M. Hagelstein, H. Förster

Deuteration of methane as a test reaction on Pt dispersion in mazzite zeolites and alumina based isomerization catalysts Original Research Article
Pages 781-788
A. Khodakov, Y. Berthier, J. Oudar, N. Barbouth, Ph. Schulz

Characterization of transition-metal ion-exchanged zeolites by NMR and EPR spectroscopy Original Research Article
Pages 789-796
S.B. Liu, T.C. Yang, R.Y. Lin, E.C. Hong, T.S. Lin

Photoacoustic Spectroscopic Study of Cobalt Containing Molecular Sieves Original Research Article
Pages 797-804
Hyun-Sik Han, Hakze Chon

Electron Spin Echo Modulation Spectroscopic Evidence for Framework Substitution of Ni(I) in NiAPSO-11 Original Research Article
Pages 805-812
Naoto Azuma, Chul Wee Lee, Maggie Zamadics, Larry Kevan

Catalytic Properties of VPI-5 Encaged Ironphthalocyanines Original Research Article
Pages 813-820
Rudy F. Parton, Cvetana P. Bezoukhanova, Frédéric Thibault-Starzyk, Reinoud A. Reynders, Piet J. Grobet, Pierre A. Jacobs

Location and photostability of faujasite-incorporated methylene blue Original Research Article
Pages 821-827
R. Hoppe, G. Schulz-Ekloff, D. Wohrle, Ch. Kirschhock, H. Fuess

Optical, electric and photoelectric properties of pure and CdS or CuCI cluster doped zeolite single crystals Original Research Article
Pages 829-836
Yu.A. Barnakov, M.S. Ivanova, V.P. Petranovskii, V.V. Poborchii, V.G. Soloviev

Zeolite MCM-22: Synthesis, Dealumination and Structural Characterization Original Research Article
Pages 37-44
S. Unverricht, M. Hunger, S. Ernst, H.G. Karge, J. Weitkamp

Magnetic and Optical Properties of Alkali Metal Clusters Inlta Original Research Article
Pages 837-842
Yasuo Nozue, Tetsuya Kodaira, Satoshi Ohwashi, Nozomu Togasffl, Taro Monji, Osamu Terasaki

Polar arenes in faujasites Original Research Article
Pages 843-850
C. Kirschhock, H. Fuess

Inelastic neutron scattering and molecular dynamics simulations of water adsorbed in the molecular sieves AIP04-11, AIP04-5, AIP04-8, and VPI-5 Original Research Article
Pages 851-858
F. Trouw, L.E. Iton, M.E. Davis

Insight into the pore structure of zeolite MCM-22 through catalytic tests. Original Research Article
Pages 859-866
A. Corma, C. Corell, A. Martinez, J. Pérez-Pariente

Study of Catalytic Properties of SAPO-40 Original Research Article
Pages 867-874
J.P. Lourenco, M.F. Ribeiro', F.R. Ribeiro, J. Rocha, Z. Gabelica, N. Dumont, E.G. Derouane

New Methods for Characterization of the External Surface of ZSM-5-Zeolites Original Research Article
Pages 875-882
K.M. Keskinen, T.T. Pakkanen, P. Raulo, M. Ruotsalainen, P. Sarv, M. Tutta

Dielectric Relaxation in Na-MFI Zeolite Original Research Article
Pages 883-890
F. Fernández-Gutierrez, M. Hernández-Velez, R. Roque-Malherbe

Molecular sieves from pillaring of layered silicates Original Research Article
Pages 45-52
She-Tin Wong, Shen-Hwa Wong, Shang-Bin Liu, Soofin Cheng

Development of a formation mechanism for M41S materials Original Research Article
Pages 53-60
J.C. Vartuli, K.D. Schmitt, C.T. Kresge, W.J. Roth, M.E. Leonowicz, S.B. McCullen, S.D. Hellring, J.S. Beck, J.L. Schlenker, D.H. Olson, E.W. Sheppard

Synthesis of Al-Containing MCM-41 Materials: Template Interaction and Removal Original Research Article
Pages 61-68
Ralf Schmidt, Duncan Akporiayea, Michael Stöcker, Ole Henrik Ellestad

Preparation and properties of Ti-containing MCM-41 Original Research Article
Pages 69-75
A. Corma, M.T. Navarro, J. Pérez-Pariente, F. Sánchez

New mesoporous titanosilicate molecular sieve Original Research Article
Pages 77-84
O. Franke, J. Rathousky, G. Schulz-Ekloff, J. Stárek, A. Zukal

Amorphous mesoporous silica-alumina with controlled pore size as acid catalysts Original Research Article
Pages 85-92
G. Bellussi, C. Perego, A. Carati, S. Peratello, E. Previde Massara, G. Perego

Nonaqueous Synthesis of Large Zeolite and Molecular Sieve Crystals Original Research Article
Pages 93-100
Suzan Nadimi, Scott Oliver, Alex Kuperman, Alan Lough, Geoffrey A. Ozin, Juan M. Garcés, Michael M. Olken, Philip Rudolf

Diversity of the system Ga2O3P2O5-H2O-HF in the presence of Organic Species Original Research Article
Pages 101-108
C. Schott-Darie, H. Kessler, M. Soulard, V. Gramlich, E. Benazzi

Convenient synthesis of crystalline microporous transition metal silicates using complexing agents Original Research Article
Pages 109-116
Rajiv Kumar, Anuj Raj, Sujit Baran Kumar, Paul Ratnasamy

Simultaneous occurrence of differently coordinated framework heteroatoms in one zeolite: MFI type vanadium silicalite, KVS-5. Original Research Article
Pages 117-124
J. Kornatowski, B. Wichterlová, M. Rozwadowski, W.H. Baur

Synthesis and characterization of highly ordered mesoporous material; FSM-16, from a layered polysilicate Original Research Article
Pages 125-132
S. Inagaki, Y. Fukushima, K. Kuroda

Zeolite Synthesis Using Catalytic Amounts of Template: Structure Blocking Effects and Stoichiometric Syntheses Original Research Article
Pages 133-140
J.L. Casci

Synthesis of high-silica zeolites with unidirectional medium pores systems using nitrogen-free templates. Original Research Article
Pages 141-146
Girolamo Giordano, Francesco Di Renzo, Françoise Remoueé, François Fajula, Dominique Plee, Philippe Schulz

Nucleation Gels for the Synthesis of Faujasite Type Zeolites Original Research Article
Pages 147-154
H. Lechert, P. Staelin, M. Wrobel, U. Schimmel

Synthesis of Omega Zeolite Without use of Tetramethylammonium(TMA) Ions Original Research Article
Pages 155-162
S. Yang, N.P. Evmiridis

Synthesis of Aluminium-rich Zeolite Beta Original Research Article
Pages 163-170
F. Vaudry, F. di Renzo, F. Fajula, P. Schulz

The influence of alkali cation on the synthesis of zeolite beta from fluoride containing gels Original Research Article
Pages 171-178
R. Mostowicz, F. Testa, F. Crea, A. Nastro, R. Aiello, A. Fonseca, J.B. Nagy

In situ studies of zeolite syntheses using powder diffraction methods. Crystallization of “instant zeolite A” powder and synthesis of CoAPO-5. Original Research Article
Pages 179-186
Poul Norby, Axel Nørlund Christensen, Jonathan C. Hanson

In-situ observation of crystal growth of silicalite under hydrothermal synthesis condition Original Research Article
Pages 187-194
T. Sano, S. Sugawara, Y. Kawakami, A. lwasaki, M. Hirata, I. Kudo, M. Ito, M. Watanabe

Zeolite ZSM-5 synthesized in the extremely dense system Original Research Article
Pages 195-202
Li Jianquan, Liu Guanghuan, Dong Jinxiang, Do Tao, Tomoyuki Inui

Ammonium-Based Alkaline-Free Synthesis of MFI-Type Boron- and Titanium Zeolites Original Research Article
Pages 203-210
U. Müller, W. Steck

On the synthesis and characterization of Cr-silicalite-1 Original Research Article
Pages 211-218
N. van der Puil, Widyawati, J.C. Jansen, H. van Bekkum

New Insights into the Mode of Formation of AIPO4-n Molecular Sieves Original Research Article
Pages 219-225
Scott Oliver, Alex Kuperman, Alan Lough, Geoffrey A. Ozin, Juan M. Garcés, Michael M. Olken, Phillip Rudolf

Synthesis and characterisation of SnAPO-5 Original Research Article
Pages 227-234
Kristin Vinje, Karl Petter Lillerud

Reverse Micelle Based Synthesis of Microporous Materials in Hydrocarbon Solvents Original Research Article
Pages 235-242
P.K. Dutta, M. Jakupca, L. Salvati, K.S.N. Reddy, R.R. Ansari

Aluminum Incorporation in Mesoporous Molecular Sieves Original Research Article
Pages 243-250
M. Janicke, D. Kumar, G.D. Stucky, B.F. Chmelka

A Novel Lead Titanate Microporous Crystal with Nanometer Size Original Research Article
Pages 251-258
Yanghong Guo, Shilun Qiu, Wenqin Pang, Naoyuki Ohnishi, Kenji Hiraga

Electron diffraction and infrared spectroscopy of amorphous aluminosilicate gels Original Research Article
Pages 259-266
B. Subotić, A.M. Tonejc, D. Bagović, A. Čižmek, T. Antonić

Some Aspects of the Preparation and Catalytic Activity of Chromia Pillared Montmorillonite Original Research Article
Pages 267-274
M. Sychev, V.H.J de Beer, R.A. Van Santen, R. Prihod'ko, V. Goncharuk

Aluminium-free layered silicates as a basic system for the preparation of pillared clays Original Research Article
Pages 275-282
W. Schwieger, K. Ponl, U. Brenn, H.G. Karge

Synthesis and MAS-NMR analysis of highly stable pillared clays Original Research Article
Pages 283-290
Juan Espinosa, Sergio Gómez, Gustavo A. Fuentes

Influence of crystalline seeds on the zeolitization of volcanic ashes: a calorimetric study Original Research Article
Pages 291-298
G.N. Kirov, N. Petrova

The formation of analcime from laumontite in the Smrekovec volcanics, Northwest Slovenia - an experimental approach Original Research Article
Pages 299-305
U. Barth-Wirsching, D. Klammer, P. Kovic-Kralj

Oriented coatings of silicalite-1 for gas sensor applications Original Research Article
Pages 307-314
J.H. Koegler, H.W. Zandbergen, J.L.N. Harteveld, M.S. Nieuwenhuizen, J.C. Jansen, H. van Bekkum

Synthesis and Characterization of A Novel Mcroporous Boron-Aluminium Chloride With A Cationic Framework Original Research Article
Pages 315-322
Jihong Yu, Kungang Tu, Ruren Xu

Use of Diels-Alder Derived Templates to Prepare Zeolites with Multidimensional Pore Systems Original Research Article
Pages 323-330
Y. Nakagawa

Synthesis, Characterization and Catalytic properties of Zeolite PSH-3/MCM-22. Original Research Article
Pages 331-338
R. Ravishankar, Tapas Sen, Veda Ramaswamy, H.S. Soni, S. Ganapathy, S. Sivasanker.

Advances in Powder Diffraction Methods for Zeolite Structure Analysis Original Research Article
Pages 341-356
Lynne B. McCusker

Low-Temperature 1H MAS NMR Investigations on the Nature of Acid Sites Causing Enhanced Catalytic Activity in H-Zeolites Original Research Article
Pages 357-364
E. Brunner, K. Beck, M. Koch, H. Pfeifer, B. Staudte, D. Zscherpel

Brönsted acidity in US-Y zeolites Original Research Article
Pages 365-372
M.A. Makarova, A. Garforth, V.L. Zholobenko, J. Dwyer, G.J. Earl, D. Rawlence

Acidic properties of metal substituted aluminophosphates studied by adsorption calorimetry and IR spectroscopy Original Research Article
Pages 373-380
J. Jänchen, M.J. Haanepen, M.P.J. Peeters, J.H.M.C. van Wolput, J.P. Wolthuizen, J.H.C. Van Hooff

Multinuclear NMR studies of acid sites in zeolites Original Research Article
Pages 381-385
H. Ernst, D. Freude, H. Pfeifer, I. Wolf

Tracing the production of spinel based ceramics from the heat induced transformations of zinc and cobalt exchanged zeolite-A using combined XRD/XAFS techniques. Original Research Article
Pages 387-394
Lorna M. Colyer, G. Neville Greaves, Andrew J. Dent, Stuart W. Carr, Katharine K. Fox, Richard H. Jones

Synthesis and characterization by X-ray diffraction and solid state NMR of ULM-5, a new fluorinated gallophosphate Ga16(P04)14(HP04)2(OH)2F7. 4 H3N(CH2)6NH3. 6 H20 with 16-membered rings. Original Research Article
Pages 395-402
T. Loiseau, D. Riou, F. Taulelle, G. Férey

Framework Fe Sites in Sodalite: A Model for Fe T Sites in Zeolites Original Research Article
Pages 403-412
D. Goldfarb, M. Bernardo, K.G. Strohmaier, D.E.W. Vaughan, H. Thomann

Microporous Titanosilicate ETS-10: Electron Microscopy Study Original Research Article
Pages 413-420
T. Ohsuna, O. Terasaki, D. Watanabe, M.W. Anderson, S. Lidin

Exploring Cation Siting in Zeolites by Solid-State NMR of Quadrupolar Nuclei Original Research Article
Pages 421-428
G. Engelhardt, M. Hunger, H. Koller, J. Weitkamp

An In-situ X-ray and NMR Study of the Formation of Layered Mesophase Materials Original Research Article
Pages 429-434
L.M. Bull, D. Kumar, S.P. Millar, T. Besier, M. Janicke, G.D. Stucky, B.F. Chmelka

Rub-10, a boron containing analogue of zeolite Nu-1. Original Research Article
Pages 435-443
U. Oberhagemann, B. Marler, I. Topalovic, H. Gies

Structural analysis by neutron diffraction of simples gases(H2, Ar, CH4and CF4) sorbed phases in AIPO4-5. Original Research Article
Pages 445-452
J.P. Coulomb, C. Martin, Y. Grillet, N. Tosi-Pellenq

Temperature Program Desorption and Reduction Studies of Octahedral Molecular Sieves Original Research Article
Pages 453-460
Y.-G. Yin, W.-Q. Xu, R. DeGuzman, Y.-F. Shen, S.L. Suib, C.-L O'Young

Effect of the stacking probability on the properties of the molecular sieves CIT-1, SSZ-26 and SSZ-33. Original Research Article
Pages 461-468
R.F. Lobo, S.I. Zones, M.E. Davis

Muon Spin Relaxation Studies of Cyclohexadienyl Radicals in Nausy Original Research Article
Pages 469-475
M. Shelley, D.J. Arseneau, M. Senba, J.J. Pan, R. Snooks, S.R. Kreitzman, D.G. Fleming, E. Roduner

Factors affecting the UV-Transparency of Molecular Sieves Original Research Article
Pages 477-483
S. Engel, U. Kynast, K.K. Unger, F. Schüth

The Study of the Surface Topography of Microporous Materials Using Atomic Force Microscopy Original Research Article
Pages 485-492
M.L. Occelli, S.A.C. Gould, G.D. Stucky

Time Dependence of Vibrational Relaxation of Deuterated Hydroxyls in Acidic Zeolites. Original Research Article
Pages 493-500
Mischa Bonn, Marco J.P. Brugmans, Aart W. Kleyn, Rutger A. Van Santen, Ad Lagendijk

Characterization of Titanium Silicalites Using Cyclic Voltammetry Original Research Article
Pages 501-508
S. de Castro-Martins, A. Tuel, Y. Ben Taârit

Copper exchanged zeolites studied with 13C and 129Xe NMR of adsorbed carbon monoxide and xenon Original Research Article
Pages 509-517
M. Hartmann, B. Boddenberg

Two-Dimensional 29Xe Exchange NMR Measurements of Xenon Dynamics in Na-A Zeolite Original Research Article
Pages 519-526
M. Janicke, B.F. Chmelka, R.G. Larsen, J. Shore, K. Schmidt-Rohr, L. Emsley, H. Long, A. Pines

Electron Transfer Reactions in H-Mordenite Original Research Article
Pages 527-534
R. Crockett, E. Roduner

Faults, Intergrowths and Random Phases in the ABC-D6R Family of Zeolites Original Research Article
Pages 535-542
R. Szostak, K.P. Lillerud

Systematic Relationships Between the Structures of CHA, AEI and KFI. Original Research Article
Pages 543-550
Karl Petter Lillerud, Duncan Akporiaye

The essential identity of the framework structures of ZSM-8 and ZSM-5 Original Research Article
Pages 551-558
C. Weidenthaler, R.X. Fischer, R.D. Shannon

Orthorhombic and monoclinic silicalites: structure, morphology, vibrational properties and crystal defects. Original Research Article
Pages 559-566
G.L. Marra, G. Tozzola, G. Leofanti, M. Padovan, G. Petrini, F. Genoni, B. Venturelli, A. Zecchina, S. Bordiga, G Ricchiardi

Deformation Analysis of the D8R-Unit in Zeolite Structures Original Research Article
Pages 567-574
Anna Bieniok, Hans-Beat Burgi

Systematic evaluation and classification of zeolite frameworks based on constituent sheets. Original Research Article
Pages 575-582
D.E. Akporiaye

Generation of 4-connected 3-dimensional nets using complex nodes Original Research Article
Pages 583-588
Kriemhild Reinecke

Si, Al Distribution in Zeolite Frameworks with Special Reference To Dempseys Rule Original Research Article
Pages 589-596
Mitsuo Sato, Koji Maeda, Keniti Hirasawa

Crystalline Galliosilicates with the Natrolite Structure Original Research Article
Pages 597-604
M.L. Occelli, E. Goldish, H. Eckert

Synthesis and Characterization of an Aluminophosphate Material With A1PO-15 Framework Type Structure Original Research Article
Pages 605-612
N. Bilba, A. Azzouz, N. Naum, D. Nibou

Modifications of structure and Si environment upon heating of SAPO-5, SAPO-34 and SAPO-37 Original Research Article
Pages 613-620
M. Briend, M.J. Peltre, P. Massiani, P.P. Man, R. Vomscheid, M. Derewinski, D. Barthomeuf

The Structure of a Krypton Encapsulate of Zeolite A Original Research Article
Pages 621-628
Nam Ho Heo, Kee Heon Cho, Karl Seff