Standard Methods for the Analysis of Oils, Fats and Derivatives

Content: 
Front Matter, Page iii
Copyright, Page iv
COMMISSION ON OILS, FATS AND DERIVATIVES, Page v
Foreword, Page vii
The Commission on Oils, Fats and Derivatives of the I.U.P.A.C., Pages ix-xiii
Warning, Page xvii
1.001 - Preparation of the Sample for Analysis, Page 2
1.101 - Determination of the Impurities, Pages 4-5
1.111 - Grinding, Page 6
1.121 - Determination of Moisture and Volatile Matter Content, Page 8
1.122 - Determination of Oil Content (Extraction Method), Pages 9-11
1.151 - Determination of Acidity of Oil, Page 14
2.001 - Preparation of the Sample, Pages 16-17
2.101 - Determination of the Density, Pages 20-22
2.102 - Determination of the Refractive Index, Pages 23-24
2.103 - Spectrophotometric Determination of the Colour, Pages 25-32
2.121 - Determination of Solidification Point of Water-Insoluble Fatty Acids (Titre), Pages 33-35
2.131 - Determination of the Bömer Value (B.V.), Pages 36-40
2.132 - Determination of the Cooling Curve of Fats, Pages 41-43
2.141 - Determination of the Dilatation of Fats, Pages 44-50
2.201 - Determination of the Acid Value (A. V.) and the Acidity, Pages 52-55
2.202 - Determination of the Saponification Value (S.V.), Pages 56-59
2.203 - Determination of the Ester Value (E.V.), Page 60
2.204 - Determination of Volatile Acids, Pages 61-65
2.205 - Determination of the Iodine Value (I.V.), Pages 66-70
2.206 - Determination of Di- and Tri-Unsaturated Fatty Acids by Ultraviolet Spectrophotometry, Pages 71-75
2.207 - Determination of Content of Isolated trans-Unsaturated Compounds by Infrared Spectrophotometry, Pages 76-79
2.208 - Determination of trans-Octadecenoic Acids by Thin-Layer Chromatography and Gas-Liquid Chromatography, Pages 80-83
2.210 - Determination of Fatty Acids in the 2-Position in the Triglycerides of Oils and Fats, Pages 84-88
2.241 - Determination of the Hydroxyl Value (OH. V.), Pages 89-91
2.251 - Determination of Epoxy-Group Oxygen, Pages 92-93
2.301 - Preparation of the Fatty Acid Methyl Esters, Pages 96-102
2.302 - Gas-Liquid Chromatography of Fatty Acid Methyl Esters, Pages 103-108
2.321 - Determination of Mono-, Di- and Triglycerides by Column Chromatography, Pages 109-113
2.322 - Determination of Monoglycerides, Pages 114-116
2.401 - Determination of the Unsaponifiable Matter, Pages 118-122
2.402 - Qualitative Examination and Determination of the Total Sterols by Their Digitonides, Pages 123-125
2.403 - Identification and Determination of Sterols by Gas-Liquid Chromatography, Pages 126-130
2.421 - Determination of Phosphorus, Pages 131-132
2.422 - Determination of the Phosphoric Acid Test (PAT) Value of Raw Linseed Oil, Pages 133-135
2.501 - Determination of the Peroxide Value (P.V.), Pages 138-139
2.502 - Determination of the “Oxidized Acids” (Insolubilization Method), Pages 140-142
2.504 - Determination of the p-Anisidine Value (p-A.V.), Pages 143-144
2.505 - Evidence of Purity and Deterioration from Ultraviolet Spectrophotometry, Pages 145-146
2.506 - Determination of Stability (the Modified “Swift Test”), Pages 147-149
2.601 - Determination of the Moisture and Volatile Matter, Pages 152-153
2.602 - Determination of Water (Entrainment Method), Pages 154-156
2.603 - Determination of Small Quantities of Water (Modified Karl Fischer Method), Pages 157-159
2.604 - Determination of the Insoluble Impurities, Pages 160-161
2.605 - Determination of Ash Content, Pages 162-163
2.621 - Detection of Propyl-, Octyl- and Dodecyl-Gallates, Butylated Hydroxyanisole and Butylated Hydroxytoluene, Pages 164-166
2.622 - Determination of Butylated Hydroxyanisole and Butylated Hydroxytoluene, Pages 167-170