Organic Functional Group Analysis. Theory and Development

Content: 
ORGANIC FUNCTIONAL GROUP ANALYSIS, Page ii
Front Matter, Page iii
Copyright, Page iv
Preface, Pages ix-x
CHAPTER 1 - Determination of the Carbonyl Group: Oximation and Other Methods, Pages 3-20
CHAPTER 2 - Analysis of Enolic-type Compounds: Kurt Meyer Bromination and Nonaqueous Titration, Pages 21-29
CHAPTER 3 - Determination of the Hydroxyl and Amino Groups: Base-catalyzed Acylation Methods, Pages 30-44
CHAPTER 4 - Determination of Hydroxyl Groups and Alkoxysilanes: Acid-catalyzed Acetylation Methods, Pages 45-59
CHAPTER 5 - Determination of the Epoxide Group: Quantitative Ring Opening Methods, Pages 60-69
CHAPTER 6 - Determination of 1,3-Dienes: Diels-Alder Addition Methods, Pages 70-79
CHAPTER 7 - Determination of Electron-rich Compounds: Electron-Donor-Acceptor Complexes and Charge Transfer Spectra, Pages 80-94
Introduction to PART II, Page 95
CHAPTER 1 - The Determination of Aldehydes in Oil of Lemon, Pages 97-99
CHAPTER 2 - The Estimation of Aldehydes and Ketones by Means of Hydroxylamine, Pages 100-101
CHAPTER 3 - Improved Hydroxylamine Method for the Determination of Aldehydes and Ketones Displacement of Oxime Equilibria by Means of Pyridine, Pages 102-107
CHAPTER 4 - Determination of Carbonyl Compounds, Pages 108-114
CHAPTER 5 - Macro- and Semimicrodetermination of Aldehydes and Ketones by Reaction with Hydroxylammonium Formate, Pages 115-119
CHAPTER 6 - Studies on the Mechanism of Oxime and Semicarbazone Formation, Pages 120-130
CHAPTER 7 - O-Methyloximes as Carbonyl Derivatives in Gas Chromatography, Mass Spectrometry, and Nuclear Magnetic Resonance, Pages 131-134
CHAPTER 8 - Quantitative Aspects of the Base-catalysed Halogenation of Aliphatic Ketones. Part I. lodination of Methyl Ketones, Pages 135-141
CHAPTER 9 - An Improved Kurt Meyer Titration, Pages 142-146
CHAPTER 10 - Nuclear Magnetic Resonance Signals from/a Tautomeric Mixture, Pages 147-150
CHAPTER 11 - Titration of Enols and Imides in Nonaqueous Solvents, Pages 151-156
CHAPTER 12 - Quantitative Ester Formation and the Determination of Alcohols and Phenols, Pages 157-159
CHAPTER 13 - Determining the Hydroxyl Content of Certain Organic Compounds Macro- and Semimicromethods, Pages 160-164
CHAPTER 14 - The Hydrolysis of Acetic Anhydride. Part III. The Catalytic Efficiency of a Series of Tertiary Amines, Pages 165-172
CHAPTER 15 - Determination of Hydroxy and Amino Compounds Using Pyromellitic Dianhydride, Pages 173-177
CHAPTER 16 - A Study of Base-catalyzed and Salt-catalyzed Acetylation of Hydroxyl Groups, Pages 178-190
CHAPTER 17 - The Detection and Estimation of the Relative Amounts of Primary and Secondary Hydroxyl Groups using N.M.R., Pages 191-196
CHAPTER 18 - Phosphoric Acetylation of the Hydroxyl Group, Pages 197-204
CHAPTER 19 - Acid-catalyzed Acetylation of Organic Hydroxyl Groups, Pages 205-215
CHAPTER 20 - 1,2-Dichloroethane as a Solvent for Perchloric Acid-catalyzed Acetylation, Pages 216-218
CHAPTER 21 - Micro Acid-catalyzed Acetylation of Organic Hydroxyl Groups, Pages 219-224
CHAPTER 22 - Determination of Alkoxy Groups in Alkoxysilanes by Acid-catalyzed Acetylation, Pages 225-230
CHAPTER 23 - Epoxy Acids from Oleic and Elaidic Acids, Pages 231-233
CHAPTER 24 - Direct Titration of Oxirane Oxygen with Hydrogen Bromide in Acetic Acid, Pages 234-237
CHAPTER 25 - Direct Titration of Epoxy Compounds and Aziridines, Pages 238-241
CHAPTER 26 - An Improved Direct Titration of α-Epoxy Compounds using Crystal Violet as the Indicator, Pages 242-247
CHAPTER 27 - The Volumetric Determination of Anthracene with Maleic Anhydride, Pages 248-252
CHAPTER 28 - Determination of Diels-Alder Active Dienes with Tetracyanoethylene, Pages 253-261
CHAPTER 29 - Precise Determination of the Molecular Weight of Trinitrobenzene Complexes, Pages 262-268
CHAPTER 30 - A Study of the Pi Complexes of Tetracyanoethylene with Phenols, Aromatic Hydrocarbons and Aryl Ethers, Pages 269-282
CHAPTER 31 - Diphenylpicrylhydrazyl as an Organic Analytical Reagent in the Spectrophotometric Analysis of Phenols, Pages 283-292
Index, Pages 293-297