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دانلود کتاب Macroscale and Microscale Organic Experiments

دانلود کتاب آزمایش های آلی مقیاس ماکرو و مقیاس

Macroscale and Microscale Organic Experiments

مشخصات کتاب

Macroscale and Microscale Organic Experiments

ویرایش: 7 
نویسندگان:   
سری:  
ISBN (شابک) : 0841238642 
ناشر:  
سال نشر:  
تعداد صفحات: 870 
زبان: English 
فرمت فایل : PDF (درصورت درخواست کاربر به PDF، EPUB یا AZW3 تبدیل می شود) 
حجم فایل: 63 مگابایت 

قیمت کتاب (تومان) : 37,000



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توضیحاتی در مورد کتاب آزمایش های آلی مقیاس ماکرو و مقیاس

این کتاب شامل جلد 1 از 2 است و دستورالعمل‌های ایمنی آزمایشگاه‌های شیمی دانشگاهی را برای جلوگیری از حوادث برای دانشجویان و دانشجویان توضیح می‌دهد. مطالب عبارتند از: (1) "مسئولیت شما برای پیشگیری از تصادف"؛ (2) "راهنمای خطرات شیمیایی"؛ (3) "تکنیک های آزمایشگاهی توصیه شده"؛ و (4) "تجهیزات ایمنی و رویه های اضطراری." ضمائم شامل وب به عنوان منبع اطلاعات ایمنی و مواد شیمیایی ناسازگار است.


توضیحاتی درمورد کتاب به خارجی

This book contains volume 1 of 2 and describes safety guidelines for academic chemistry laboratories to prevent accidents for college and university students. Contents include: (1) "Your Responsibility for Accident Prevention"; (2) "Guide to Chemical Hazards"; (3) "Recommended Laboratory Techniques"; and (4) "Safety Equipment and Emergency Procedures." Appendices include the Web as a source of safety information and incompatible chemicals.



فهرست مطالب

Dedication
Contents
Preface
Organic Experiments and Waste Disposal
Ch 1: Introduction
	Experimental Organic Chemistry
	Equipment for Experimental Organic Chemistry
	Check-In of Lab Equipment
	Transfer of Liquids and Solids
	Weighing and Measuring
	Washing and Drying Laboratory Equipment
	Miscellaneous Cleanup
	The Laboratory Notebook
Ch 2: Laboratory Safety, Courtesy, and Waste Disposal
	Important General Rules
	Laboratory Courtesy
	Working with Flammable Substances
	Working with Hazardous Chemicals
	Working with Explosive Hazards
	Working with Corrosive Substances
	Working with Toxic Substances
	Gloves
	Using the Laboratory Hood
	Working at Reduced Pressure
	Working with Compressed Gas Cylinders
	Odoriferous Chemicals
	Waste Disposal-Cleaning Up
	Biohazards
	Questions
Ch 3: Melting Points and Boiling Points
	Part 1: Five Concepts for Predicting Physical Properties
	Part 2: Melting Points
	Part 3: Boiling Points
	Questions
	References
Ch 4: Recrystallization
	The Seven Steps of Recrystallization
	Experiments
	Recrystallization Problems and Their Solutions
	Recrystallization Summary
	Questions
Ch 5: Distillation
	Simple Distillation
	Fractional Distillation
	Liquid Mixtures
	Azeotropes
	Boiling Points and Distillation
	Experiments
	Questions
	Reference
Ch 6: Steam Distillation, Vacuum Distillation, and Sublimation
	Part 1: Steam Distillation
	Experiments
	Part 2: Vacuum Distillation
	Part 3: Sublimation
	Experiment
	Questions
Ch 7: Extraction
	Partition Coefficient
	Properties of Extraction Solvents
	Mixing and Separating the Layers
	Drying Agents
	Part 1: The Technique of Neutral Liquid/Liquid Extraction
	Experiment
	Part 2: Acid/Base Liquid/Liquid Extraction
	Experiments
	Extractions from Common Items
	Questions
Ch 8: Thin-Layer Chromatography: Analyzing Analgesics and Isolating Lycopene from Tomato Paste
	Uses of Thin-Layer Chromatography
	The Principles of Chromatography
	The Six Steps of Thin-Layer Chromatography
	Comparison of Different Types of Chromatography
	Experiments
	Discussion
	Fluorescence
	Thin-Layer Chromatography Summary
	Questions
Ch 9: Column Chromatography: Fluorenone, Cholesteryl Acetate, Acetylferrocene, and Plant Pigments
	Additional Principles of Column Chromatography
	Other Types of Chromatography
	Experiments
	Questions
Ch 10: Gas Chromatography: Analyzing Alkene Isomers
	The General GC Analysis Procedure
	Experiments
	Questions
Ch 11: Infrared Spectroscopy
	Analysis of IR Spectra
	The Fourier Transform Infrared (FTIR) Spectrometer
	Experimental Considerations
	The Spectra of Neat Liquids
	The Spectra of Solutions
	Mulls
	Potassium Bromide Disk
	Diffuse Reflectance
	Gas Phase IR Spectroscopy: The Williamson Gas Phase IR Cell
	For Further Investigation
	Experiment
	References
Ch 12: Nuclear Magnetic Resonance Spectroscopy
	Interpretation of 1H NMR Spectra
	Carbon-13 Spectroscopy
	Fourier Transform Spectroscopy
	Experiments
	Questions
	References
Ch 13: Mass Spectrometry
	The Mass Spectrometer
	Interpretation of Electron Ionization Spectra
	Gas Chromatography-Mass Spectrometry (GC-MS)
	Bioanalytical Mass Spectrometry
	Questions
	References
Ch 14: Ultraviolet Spectroscopy, Refractive Indices, and Qualitative Instrumental Organic Analysis
	Ultraviolet Spectroscopy
	Experiment
	Experiment
	Questions
	References
Ch 15: Computational Chemistry
	Graphical and Mathematical Models
	Molecular Mechanics Models
	Quantum Chemical or AB Initio Models
	Semiempirical Models
	Types of Calculations
	Examples of Calculations
	References
	The Synthetic Experiments
Ch 16: The SN2 Reaction: 1-Bromobutane
	Experiments
	Questions
Ch 17: Nucleophilic Substitution Reactions of Alkyl Halides
	Experiments
	Questions
Ch 18: Radical Initiated Chlorination of 1-Chlorobutane
	Relative Reactivates of Hydrogen
	Experiments
	Gas Chromatography
	Computational Chemistry
	Questions
Ch 19: Alkenes from Alcohols: Cyclohexene from Cyclohexanol
	Experiments
	Questions
Ch 20: Bromination and Debromination: Purification of Cholesterol
	Experiments
	Questions
Ch 21: Dichlorocarbene
	The Thermal Decomposition of Sodium Trichloroacetate; Reaction of Dichlorocarbene with 1.5-Cyclooctadiene
	Questions
Ch 22: Oxidation: Cyclohexanol to Cyclohexanone; Cyclohexanone to Adipic Acid
	The Oxidation of an Alcohol to a Ketone
	The Oxidation of a Ketone to a Carboxylic Acid
	Experiments
	Questions
Ch 23: The Cannizzaro Reaction: Simultaneous Synthesis of an Alcohol and an Acid in the Absence of Solvent
	Experiment
	Questions
Ch 24: Oxidative Coupling of Alkynes: 2,7-Dimethyl-3,5-Octadiyn-2,7-Diol
	Experiment
	Questions
Ch 25: Catalytic Hydrogenation
	Experiments
	Questions
Ch 26: Sodium Borohydride Reduction of 2-Methylcyclohexanone: A Problem in Conformational Analysis
	Experiment
	Questions
Ch 27: Epoxidation of Cholesterol
	Steroid Biosynthesis through an Epoxide Intermediate
	Experiments
	Questions
	Reference
Ch 28: Nitration of Methyl Benzoate
	Experiments
	Questions
Ch 29: Friedel-Crafts Alkylation of Benzene and Dimethoxybenzene; Host-Guest Chemistry
	Inclusion Complex: Host-Guest Chemistry
	Experiments
	Questions
Ch 30: Alkylation of Mesitylene
	Experiment
	Questions
Ch 31: The Friedel-Crafts Reaction: Anthraquinone and Anthracene
	Fieser's Solution, an Oxygen Scavenger
	Experiments
	Questions
Ch 32: Friedel-Crafts Acylation of Ferrocene: Acetylferrocene
	Experiment
	Questions
Ch 33: Reactions of Triphenylmethyl Carbocation, Carbanion, and Radical
	Experiments
	Questions
Ch 34: 1,2,3,4-Tetraphenyl-Naphthalene via Benzyne
	Experiments
	Questions
Ch 35: Triptycene via Benzyne
	Experiment
	Computational Chemistry
	Questions
Ch 36: Aldehydes and Ketones
	Reactions of the Carbonyl Group
	Bisulfite Addition
	Cyanide Addition
	Schiff Bases
	Oximes, SemicarbaZones, and 2,4-Dinitrophenylhydrazones
	Tollens' Reagent
	Schiff's Reagent
	Iodoform Test
	Experiments
	Questions
Ch 37: Dibenzalacetone by the Aldol Condensation
	Experiment
	Questions
Ch 38: Grignard Synthesis of Triphenylmethanol and Benzoic Acid
	Experiments
	Questions
Ch 39: The Wittig and Wittig-Horner Reactions
	Experiments
	Questions
Ch 40: Esterification and Hydrolysis
	Experiments
	Questions
Ch 41: Acetylsalicylic Acid (Aspirin)
	Experiment
	Questions
Ch 42: Malonic Ester of a Barbiturate
	Experiments
	Questions
Ch 43: Amines
	Experiments
	Questions
Ch 44: The Sandmeyer Reaction: 1-Bromo-4-Chlorobenzene, 2-Iodobenzoic Acid, and 4-Chlorotoluene
	Three Sandmeyer Reactions
	Experiments
	Questions
Ch 45: Synthesis and Bioassay of Sulfanilamide and Derivatives
	Part 1: The Synthesis and Bioassay of Sulfanilamide
	The Synthetic Sequence of Sulfanilamide
	Experiments
	Part 2: Synthesis and Bioassay of Sulfanilamide Derivatives
	Experiments
	Questions
Ch 46: Dyes and Dyeing
	Part 1: Dyes
	Experiments
	Part 2: Dyeing Experiments
	Questions
Ch 47: Martius Yellow
	Experiments
	Questions
Ch 48: Diels-Alder Reaction
	Experiments
	Questions
Ch 49: Ferrocene [Bis(Cyclopentadienyl)Iron]
	Experiments
	Questions
Ch 50: A Diels-Alder Reaction Puzzle: The Reaction of 2,4-Hexadien-1-ol with Maleic Anhydride
	Question
Ch 51: Tetraphenylcyclopentadienone
	Experiments
	Question
Ch 52: Hexaphenylbenzene and Dimethyl Tetraphenylphthalate
	Experiments
	Computational Chemistry
	Questions
	Derivatives of 1,2-Diphenylethane: A Multistep Synthesis
Ch 53: The Benzoin Condensation: Catalysis by the Cyanide Ion and Thiamine
	Experiments
	Questions
Ch 54: Nitric Acid Oxidation; Preparation of Benzil from Benzoin; and Synthesis of a Heterocycle: Diphenylquinoxaline
	Experiments
	Questions
Ch 55: The Borohydride Reduction of a Ketone: Hydrobenzoin from Benzil
	Experiment
	Questions
Ch 56: The Synthesis of 2,2-Dimethyl-1,5-Dioxolane; The Acetonide Derivative of a Vicinal Diol
	Experiment
	Questions
Ch 57: 1,4-Addition: Reductive Acetylation of Benzil
	Experiments
	Computational Chemistry
Ch 58: The Synthesis of an Alkyne from an Alkene by Bromination and Dehydrobromination: Stilbene and Diphenylacetylene
	Experiments
	Questions
Ch 59: The Perkin Reaction: Synthesis of a-Phenylcinnamic Acid and Its Decarboxylation to cis-Stilbene
	Experiments: Part 1
	Decarboxylation: Synthesis of cis - Stilbene
	Experiments: Part 2
	Computational Chemistry
	Questions
Ch 60: Multicomponent Reactions: The Aqueous Passerini Reaction
	The Aqueous Passerini Reaction
	Questions
Ch 61: Chemiluminescence: Syntheses of Cyalume and Luminol
	Cyalume
	Luminol
	Experiments
Ch 62: Photochemistry: The Synthesis of Benzopinacol
	Experiments
	Questions
Ch 63: Carbohydrates and Sweeteners
	Sweeteners
	Analysis of Carbohydrates
	Experiments
	Questions
Ch 64: Virstatin, a Possible Treatment for Cholera
	Questions
Ch 65: Biosynthesis of Ethanol and Enzymatic Reactions
	Experiments
	Part 2. Enzymatic Reactions: A Chiral Alcohol from a Ketone
	Experiments
	Questions
Ch 66: The Synthesis of Natural Products: The Sex Attractant of the Cockroach and Camphor
	Part 1: The Synthesis of the Sex Attractant of the German Cockroach
	Part 2: The Conversion of Camphene to Camphor
	Experiments
	Questions
Ch 67: Polymers: Synthesis and Recycling
	Part 1: Synthesis of Polymers
	Experiments
	Part 2: Recycling Plastics
	Experiments
	Questions
	Agricultural Science Module
	Food Science Module
	Textile Module
	Forensics Module
	Chrysanthemic Acid: A Team Project
	Writing Module
Ch 68: Searching the Chemical Literature
	Looking for Information on a Specific Compound
	Looking to Plan Synthesis
	Looking for General Information
Index




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