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دانلود کتاب Macroscale and Microscale Organic Experiments
دانلود کتاب آزمایش های آلی مقیاس ماکرو و مقیاس
مشخصات کتاب
Macroscale and Microscale Organic Experiments
ویرایش: 7
نویسندگان: Kenneth L. Williamson Katherine M. Masters
سری:
ISBN (شابک) : 0841238642
ناشر:
سال نشر:
تعداد صفحات: 870
زبان: English
فرمت فایل : PDF (درصورت درخواست کاربر به PDF، EPUB یا AZW3 تبدیل می شود)
حجم فایل: 63 مگابایت
قیمت کتاب (تومان) : 37,000
در صورت تبدیل فایل کتاب Macroscale and Microscale Organic Experiments به فرمت های PDF، EPUB، AZW3، MOBI و یا DJVU می توانید به پشتیبان اطلاع دهید تا فایل مورد نظر را تبدیل نمایند.
توجه داشته باشید کتاب آزمایش های آلی مقیاس ماکرو و مقیاس نسخه زبان اصلی می باشد و کتاب ترجمه شده به فارسی نمی باشد. وبسایت اینترنشنال لایبرری ارائه دهنده کتاب های زبان اصلی می باشد و هیچ گونه کتاب ترجمه شده یا نوشته شده به فارسی را ارائه نمی دهد.
توضیحاتی در مورد کتاب آزمایش های آلی مقیاس ماکرو و مقیاس
این کتاب شامل جلد 1 از 2 است و دستورالعمل‌های ایمنی آزمایشگاه‌های شیمی دانشگاهی را برای جلوگیری از حوادث برای دانشجویان و دانشجویان توضیح می‌دهد. مطالب عبارتند از: (1) "مسئولیت شما برای پیشگیری از تصادف"؛ (2) "راهنمای خطرات شیمیایی"؛ (3) "تکنیک های آزمایشگاهی توصیه شده"؛ و (4) "تجهیزات ایمنی و رویه های اضطراری." ضمائم شامل وب به عنوان منبع اطلاعات ایمنی و مواد شیمیایی ناسازگار است.
توضیحاتی درمورد کتاب به خارجی
This book contains volume 1 of 2 and describes safety guidelines for academic chemistry laboratories to prevent accidents for college and university students. Contents include: (1) "Your Responsibility for Accident Prevention"; (2) "Guide to Chemical Hazards"; (3) "Recommended Laboratory Techniques"; and (4) "Safety Equipment and Emergency Procedures." Appendices include the Web as a source of safety information and incompatible chemicals.
فهرست مطالب
Dedication Contents Preface Organic Experiments and Waste Disposal Ch 1: Introduction Experimental Organic Chemistry Equipment for Experimental Organic Chemistry Check-In of Lab Equipment Transfer of Liquids and Solids Weighing and Measuring Washing and Drying Laboratory Equipment Miscellaneous Cleanup The Laboratory Notebook Ch 2: Laboratory Safety, Courtesy, and Waste Disposal Important General Rules Laboratory Courtesy Working with Flammable Substances Working with Hazardous Chemicals Working with Explosive Hazards Working with Corrosive Substances Working with Toxic Substances Gloves Using the Laboratory Hood Working at Reduced Pressure Working with Compressed Gas Cylinders Odoriferous Chemicals Waste Disposal-Cleaning Up Biohazards Questions Ch 3: Melting Points and Boiling Points Part 1: Five Concepts for Predicting Physical Properties Part 2: Melting Points Part 3: Boiling Points Questions References Ch 4: Recrystallization The Seven Steps of Recrystallization Experiments Recrystallization Problems and Their Solutions Recrystallization Summary Questions Ch 5: Distillation Simple Distillation Fractional Distillation Liquid Mixtures Azeotropes Boiling Points and Distillation Experiments Questions Reference Ch 6: Steam Distillation, Vacuum Distillation, and Sublimation Part 1: Steam Distillation Experiments Part 2: Vacuum Distillation Part 3: Sublimation Experiment Questions Ch 7: Extraction Partition Coefficient Properties of Extraction Solvents Mixing and Separating the Layers Drying Agents Part 1: The Technique of Neutral Liquid/Liquid Extraction Experiment Part 2: Acid/Base Liquid/Liquid Extraction Experiments Extractions from Common Items Questions Ch 8: Thin-Layer Chromatography: Analyzing Analgesics and Isolating Lycopene from Tomato Paste Uses of Thin-Layer Chromatography The Principles of Chromatography The Six Steps of Thin-Layer Chromatography Comparison of Different Types of Chromatography Experiments Discussion Fluorescence Thin-Layer Chromatography Summary Questions Ch 9: Column Chromatography: Fluorenone, Cholesteryl Acetate, Acetylferrocene, and Plant Pigments Additional Principles of Column Chromatography Other Types of Chromatography Experiments Questions Ch 10: Gas Chromatography: Analyzing Alkene Isomers The General GC Analysis Procedure Experiments Questions Ch 11: Infrared Spectroscopy Analysis of IR Spectra The Fourier Transform Infrared (FTIR) Spectrometer Experimental Considerations The Spectra of Neat Liquids The Spectra of Solutions Mulls Potassium Bromide Disk Diffuse Reflectance Gas Phase IR Spectroscopy: The Williamson Gas Phase IR Cell For Further Investigation Experiment References Ch 12: Nuclear Magnetic Resonance Spectroscopy Interpretation of 1H NMR Spectra Carbon-13 Spectroscopy Fourier Transform Spectroscopy Experiments Questions References Ch 13: Mass Spectrometry The Mass Spectrometer Interpretation of Electron Ionization Spectra Gas Chromatography-Mass Spectrometry (GC-MS) Bioanalytical Mass Spectrometry Questions References Ch 14: Ultraviolet Spectroscopy, Refractive Indices, and Qualitative Instrumental Organic Analysis Ultraviolet Spectroscopy Experiment Experiment Questions References Ch 15: Computational Chemistry Graphical and Mathematical Models Molecular Mechanics Models Quantum Chemical or AB Initio Models Semiempirical Models Types of Calculations Examples of Calculations References The Synthetic Experiments Ch 16: The SN2 Reaction: 1-Bromobutane Experiments Questions Ch 17: Nucleophilic Substitution Reactions of Alkyl Halides Experiments Questions Ch 18: Radical Initiated Chlorination of 1-Chlorobutane Relative Reactivates of Hydrogen Experiments Gas Chromatography Computational Chemistry Questions Ch 19: Alkenes from Alcohols: Cyclohexene from Cyclohexanol Experiments Questions Ch 20: Bromination and Debromination: Purification of Cholesterol Experiments Questions Ch 21: Dichlorocarbene The Thermal Decomposition of Sodium Trichloroacetate; Reaction of Dichlorocarbene with 1.5-Cyclooctadiene Questions Ch 22: Oxidation: Cyclohexanol to Cyclohexanone; Cyclohexanone to Adipic Acid The Oxidation of an Alcohol to a Ketone The Oxidation of a Ketone to a Carboxylic Acid Experiments Questions Ch 23: The Cannizzaro Reaction: Simultaneous Synthesis of an Alcohol and an Acid in the Absence of Solvent Experiment Questions Ch 24: Oxidative Coupling of Alkynes: 2,7-Dimethyl-3,5-Octadiyn-2,7-Diol Experiment Questions Ch 25: Catalytic Hydrogenation Experiments Questions Ch 26: Sodium Borohydride Reduction of 2-Methylcyclohexanone: A Problem in Conformational Analysis Experiment Questions Ch 27: Epoxidation of Cholesterol Steroid Biosynthesis through an Epoxide Intermediate Experiments Questions Reference Ch 28: Nitration of Methyl Benzoate Experiments Questions Ch 29: Friedel-Crafts Alkylation of Benzene and Dimethoxybenzene; Host-Guest Chemistry Inclusion Complex: Host-Guest Chemistry Experiments Questions Ch 30: Alkylation of Mesitylene Experiment Questions Ch 31: The Friedel-Crafts Reaction: Anthraquinone and Anthracene Fieser's Solution, an Oxygen Scavenger Experiments Questions Ch 32: Friedel-Crafts Acylation of Ferrocene: Acetylferrocene Experiment Questions Ch 33: Reactions of Triphenylmethyl Carbocation, Carbanion, and Radical Experiments Questions Ch 34: 1,2,3,4-Tetraphenyl-Naphthalene via Benzyne Experiments Questions Ch 35: Triptycene via Benzyne Experiment Computational Chemistry Questions Ch 36: Aldehydes and Ketones Reactions of the Carbonyl Group Bisulfite Addition Cyanide Addition Schiff Bases Oximes, SemicarbaZones, and 2,4-Dinitrophenylhydrazones Tollens' Reagent Schiff's Reagent Iodoform Test Experiments Questions Ch 37: Dibenzalacetone by the Aldol Condensation Experiment Questions Ch 38: Grignard Synthesis of Triphenylmethanol and Benzoic Acid Experiments Questions Ch 39: The Wittig and Wittig-Horner Reactions Experiments Questions Ch 40: Esterification and Hydrolysis Experiments Questions Ch 41: Acetylsalicylic Acid (Aspirin) Experiment Questions Ch 42: Malonic Ester of a Barbiturate Experiments Questions Ch 43: Amines Experiments Questions Ch 44: The Sandmeyer Reaction: 1-Bromo-4-Chlorobenzene, 2-Iodobenzoic Acid, and 4-Chlorotoluene Three Sandmeyer Reactions Experiments Questions Ch 45: Synthesis and Bioassay of Sulfanilamide and Derivatives Part 1: The Synthesis and Bioassay of Sulfanilamide The Synthetic Sequence of Sulfanilamide Experiments Part 2: Synthesis and Bioassay of Sulfanilamide Derivatives Experiments Questions Ch 46: Dyes and Dyeing Part 1: Dyes Experiments Part 2: Dyeing Experiments Questions Ch 47: Martius Yellow Experiments Questions Ch 48: Diels-Alder Reaction Experiments Questions Ch 49: Ferrocene [Bis(Cyclopentadienyl)Iron] Experiments Questions Ch 50: A Diels-Alder Reaction Puzzle: The Reaction of 2,4-Hexadien-1-ol with Maleic Anhydride Question Ch 51: Tetraphenylcyclopentadienone Experiments Question Ch 52: Hexaphenylbenzene and Dimethyl Tetraphenylphthalate Experiments Computational Chemistry Questions Derivatives of 1,2-Diphenylethane: A Multistep Synthesis Ch 53: The Benzoin Condensation: Catalysis by the Cyanide Ion and Thiamine Experiments Questions Ch 54: Nitric Acid Oxidation; Preparation of Benzil from Benzoin; and Synthesis of a Heterocycle: Diphenylquinoxaline Experiments Questions Ch 55: The Borohydride Reduction of a Ketone: Hydrobenzoin from Benzil Experiment Questions Ch 56: The Synthesis of 2,2-Dimethyl-1,5-Dioxolane; The Acetonide Derivative of a Vicinal Diol Experiment Questions Ch 57: 1,4-Addition: Reductive Acetylation of Benzil Experiments Computational Chemistry Ch 58: The Synthesis of an Alkyne from an Alkene by Bromination and Dehydrobromination: Stilbene and Diphenylacetylene Experiments Questions Ch 59: The Perkin Reaction: Synthesis of a-Phenylcinnamic Acid and Its Decarboxylation to cis-Stilbene Experiments: Part 1 Decarboxylation: Synthesis of cis - Stilbene Experiments: Part 2 Computational Chemistry Questions Ch 60: Multicomponent Reactions: The Aqueous Passerini Reaction The Aqueous Passerini Reaction Questions Ch 61: Chemiluminescence: Syntheses of Cyalume and Luminol Cyalume Luminol Experiments Ch 62: Photochemistry: The Synthesis of Benzopinacol Experiments Questions Ch 63: Carbohydrates and Sweeteners Sweeteners Analysis of Carbohydrates Experiments Questions Ch 64: Virstatin, a Possible Treatment for Cholera Questions Ch 65: Biosynthesis of Ethanol and Enzymatic Reactions Experiments Part 2. Enzymatic Reactions: A Chiral Alcohol from a Ketone Experiments Questions Ch 66: The Synthesis of Natural Products: The Sex Attractant of the Cockroach and Camphor Part 1: The Synthesis of the Sex Attractant of the German Cockroach Part 2: The Conversion of Camphene to Camphor Experiments Questions Ch 67: Polymers: Synthesis and Recycling Part 1: Synthesis of Polymers Experiments Part 2: Recycling Plastics Experiments Questions Agricultural Science Module Food Science Module Textile Module Forensics Module Chrysanthemic Acid: A Team Project Writing Module Ch 68: Searching the Chemical Literature Looking for Information on a Specific Compound Looking to Plan Synthesis Looking for General Information Index
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