Advances in Instrumentation

Front Matter....Pages I-XV
Front Matter....Pages 1-1
The Automation of Thermal Analysis Instrumentation: Thermogravimetry and Differential Thermal Analysis....Pages 3-15
Fast Differential Thermal Analysis....Pages 17-34
A New Differential Thermal Analysis System....Pages 35-43
Theoretical Consideration of Micro Sample Differential Thermal Analysis....Pages 45-54
Low Temperature DTA — A Survey....Pages 55-73
Constant Sensitivity Differential Thermal Analysis: Development and Evaluation....Pages 75-85
A New System for Sub-Ambient Temperature Differential Thermal Analysis (Range −196° to +500°C)....Pages 87-98
A Multichannel Analyser System in DTA Curves Recording....Pages 99-108
Effects of Gas Environment upon the Calorimetric Calibration Constant of DTA Cells....Pages 109-113
Zerlegbarer, universeller DTA-Meßkopf....Pages 115-125
Instrumental Limitations upon the Measurement of Temperature and Rate of Energy Production by Differential Scanning Calorimetry....Pages 127-138
The Evaluation of Catalysts by Pressure DSC....Pages 139-150
Mesures de Chaleur de Reaction en Analyse Enthalpique Differentielle....Pages 151-160
Quasi Isothermal Thermogravimetry....Pages 161-170
Simultaneous TG and X-ray Analysis Method and Applications....Pages 171-185
Accurate Thermogravimetry at Very High Temperatures....Pages 187-195
Operating Experience with a Multi-Specimen ‘Carousel’ Weighing Device....Pages 197-208
Low-Cost Micro-TG at High Rates of Heating....Pages 209-224
Application of Micro Balances to the Measurement of Gas Pressure Over Eight Decades....Pages 225-233
A Device for Simultaneous Determination of Mass Flow and Reaction Force of a Gas Stream from a Heated Sample....Pages 235-241
Front Matter....Pages 1-1
The Analysis of Thermogravimetric Curves Using an Analogue Simulation Language....Pages 243-253
Investigation of Evaporation by Thermogravimetry....Pages 255-268
Eine neue DSC-Methode....Pages 269-277
Design Considerations in Advanced Systems for Differential Scanning Calorimetry....Pages 279-294
Differential Scanning Calorimetry at 150 ATM Pressure....Pages 295-301
A New Instrument for Simultaneous DTA — Mass Spectrometric Analysis....Pages 303-312
Analyseur Thermique Pour Le Dosage Simultane Du SO 2 et du CO 2 ....Pages 313-324
Tandem Thermogravimetric Analyzer — Time-of-Flight Mass Spectrometer System Designed for Toxicological Evaluation of Nonmetallic Materials....Pages 325-336
Application of a Scan-Programmer to Control a Quadrupole Mass Spectrometer....Pages 337-342
The Calibration and Interpretation of Data from a Constant Volume Mass Spectrometer, Thermal Analysis System....Pages 343-354
Determination of Kinetic Parameters from a Single Thermogram....Pages 355-366
Neue Methode und Vorrichtung für die Reaktionskinetische Interpretation Thermogravimetrischer Messergebnisse....Pages 367-372
Activation Energy of a Thermolysis : Conditions for a Significant Measurement under Very Low Pressures....Pages 373-377
Determination of Activation Energies for Diffusion-Controlled Agglomeration Reactions in Metals by Differential Thermal Analysis....Pages 379-387
Reaction Differential Thermal Analysis....Pages 389-396
The Optimization of Instrumental Parameters in Thermal Analytical Techniques for Sensitivity, Accuracy, and Convenience of Data Presentation....Pages 397-407
How is an Acceptable Nomenclature System Achieved?....Pages 409-414
Data Acquisition in Thermal Analysis....Pages 415-424
A New Interpretation of DTA Curves at Quantitative Investigations....Pages 425-439
Peak Areas and Heats of Transition of DTA Temperature Standards....Pages 441-452
Front Matter....Pages 1-1
Easy Method for the Evaluation of Peak Areas....Pages 453-460
Apparatur für die Periodische Thermische Analyse (PTA)....Pages 461-473
A Simultaneous ETA-DTA-Equipment....Pages 475-488
Thermogastitrimetrische Untersuchung von Bauxiten....Pages 489-498
A Versatile Hot Stage Microscope Unit....Pages 499-513
Fast Characterization of Catalysts by a New Thermal Method....Pages 515-524
The Measurement of Thermal Diffusivity by Three Methods....Pages 525-538
On a Sequential Measuring System of Diffusivity vs. Temperature....Pages 539-548
Differential Thermocouple up to 2450°C and Thermographic Investigation of Refractory Silicides....Pages 549-559
The Application of Thermogravimetry to Physicochemical Investigations....Pages 561-572
A Critique on the Definition of Adsorption....Pages 573-582
On the Application of Resonating Quartz Crystals in Thermogravimetry....Pages 583-589
Requirements and Realization of Thermal Analysis Standards. Temperature Standards for DTA....Pages 591-608
Further Recommendations for Nomenclature in Thermal Analysis....Pages 609-614
Books and Monographs on Thermal Analysis Report of the Publications Committee....Pages 615-622
Back Matter....Pages 623-631